The morphology of dentinal cavity walls, wetting by poly (methyl methacrylate), and resistance to tensile forces was studied with a scanning electron microscope, before and after etching or fixation, or both, with glutaraldehyde. Results indicated that the surface layer of dentinal cavity walls after etching is of an aqueous-organic nature, that glutaraldehyde fixation improves the mechanical properties of the surface layer of the cavity wall, and that wetting by poly (methyl methacrylate) is effective.
References
1.
Phillips, R.W., and Ryge, G. (eds) : Adhesive Restorative Dental Materials, Springfield, Va: Clearinghouse, US Department of Commerce , 1961.
Driessens, F.C.M. (ed) : Dental Tissues and Materials, Nijmegen: University of Nijmegen, 1971.
4.
Eick, J.D.; Johnson, L.N.; Fromer, J.R.; Good, R.J.; and Neuman, A.W.: Surface Topography, Its Influence on Wetting and Adhesion in a Dental Adhesive System, J Dent Res51: 780-788, 1972.
5.
Retief, D.H. : The Intra-Oral Factors Affecting Adhesion , J Dent Assoc S Africa25: 392-399, 1970.
6.
Buonocore, M.G. : Principles of Adhesive Retention and Adhesive Restorative Materials, JADA67: 382-291, 1963.
7.
Salomon, G.: Adhesion and Abhesion in Biological Systems, in Driessens, F.C.M. (ed): Dental Tissues and Materials, Nijmegen: University of Nijmegen1971, p 111.
8.
Vale, W.A.: Cavity Preparations and Further Thoughts on High Speed, Br Dent J107: 333-346, 1959.
Greener, B.H. , and Lindenmeyer , R.S.: Bur Geometry and Its Relationship to Cutting , J Dent Res47: 87-97, 1968.
11.
DEWIJN, J.R.: Unpublished data, 1971.
12.
Eick, J.D.; Wilke, R.A.; Anderson, C.H.; and Sörensen, S.E.: Scanning Electron Microscopy of Cut Tooth Surfaces and Identification of Debris by Use of the Electron Microprobe, J Dent Res49: 1359-1368, 1970.
13.
Lee, H.L. , and Swartz, M.L.: Sealing of Developmental Pits and FissuresI. In Vitro Study, J Dent Res50: 133-140, 1971.
14.
Baume, L.J.: Compatibility of Some New Synthetic Materials with Host Tissues, in Driessens, F.C.M. (ed) : Dental Tissues and Materials, Nijmegen, University of Nijmegen, 1971, p 249.
15.
Analytische Methoden fur Atomabsorption und Flammenemission, Zeiss, Carl, Ca 1-1 (1968) Oberkochen , Germany.
16.
Bergman, E. , and Loxley, R.: Two Improved and Simplified Methods for the Spectrophotometric Determination of Hydroxyproline, Anal Chem35: 1961-1965, 1963.
17.
SALOMON, G.: Unpublished work, 1972.
18.
Bowes, J.H. , and Cater, C.W.: The Reaction of Glutaraldehyde with Proteins and Other Biological Materials, J Roy Microsc Soc85: 193-200, 1965.
19.
Richards, F.M. , and Knowles, J.R.: Glutaraldehyde as a Protein Crosslinking Reagent, J Molec Biol37: 231-233, 1968.
20.
Hopwood, D. : A Comparison of the Crosslinking Abilities of Glutaraldehyde, Formaldehyde and a-Hydroxyadipaldehyde with Bovine Serum and Cassein, Histochemie17: 151-161, 1969.
21.
Piez, K.A.: Maturation of Collagen, J Dent Res45: 463-468, 1966.
22.
Witte, W.E. , and Fullmer, H.M.: Effects of Age on Dentin Demonstrated with Azure A, J Dent Res46: 218-221, 1967.
23.
Bailey, A.J. ; Fowler, L.J.; and Peach, C.M.: Identification of Two Interchain Crosslinks of Bone and Dentin Collagen, Biochem Biophys Res Comm35: 663-675, 1969.
24.
Bakerman, S. : Quantitative Extraction of Acid-Soluble Human Skin Collagen with Age, Nature (Lond ) 196: 375-376, 1962.
25.
Sabatini, D.D. ; Bensch, K.; and Barnett, R.J.: The Preservation of Cellular Ultra-structure and Enzymatic Activity by Aldehyde Fixation, J Cell Biol17: 19-58, 1963.
26.
Flitney, F.W. : The Time Course of Fixation of Albumin by Formaldehyde, Glutaraldehyde, Acrolein and Other Higher Aldehydes, J Roy Microsc Soc85: 353-364, 1966.
27.
Hopwood, D.: Some Aspects of Fixation with Glutaraldehyde, J Anat101: 1: 83-92, 1967.
28.
Hopwood, D. : The Elution Pattern of Formaldehyde, Glutaraldehyde, Glyoxal and a-Hydroxyadipaldehyde from Sephadex G-10 and Their Significance for Tissue Fixation, Histochemie20: 127-132, 1969.
29.
Masuhara, E. : Über die Chemie eines neuen haftfahigen Kunststoff- Fül-lungs materials, Dtsch Zahnaertzl Z24: 620-628, 1969.
30.
Brauer, G.M. : In Vitro Reactivity of Surfaces of Calcified Tissues, in Driessens, F.C.M. (ed): Dental Tissues and Materials, Nijmegen: University of Nijmegen, 1971, p 193.
31.
Driessens, F.C.M.; Brauer, G.M.; and Termini, D.J.: Chelating Agents as Potential Adhesives for Dental Restorations, abstracted, IADR Program and Abstracts of Papers, No. 137, 1969.
32.
Dickson, G. , and Barton, J.A.: An Isotropic and Time-Dependent Variation in the Thermal Expansion of Dentin, abstracted IADR Program Abstracts of Papers, No. 860, 1972 .