Abstract
Pneumatic conveying systems have become a standard technique for the transport of bulk materials such as powdery or granulates. The spatial dependence of the material density and the stream velocity in such transport systems require a volumetric measurement principle for flow measurement. In this paper we analyse the capability to estimate the volume fraction from capacitive sensing data using electrical capacitance tomography (ECT). In particular, we investigate the capability of back-projection type imaging algorithms. The ill-posed nature of the imaging problem of ECT require the incorporation of prior knowledge in the design of the estimator. We analyse the different flow profiles in pneumatic conveying in order to generate specific sample-based prior information to improve the estimation performance and robustness. We discuss the construction of different linear image reconstruction algorithms and present a framework, which allows a detailed statistical analysis of the estimator performance. Simulation studies show the estimation behaviour of different algorithms with respect to the incorporated prior information. We demonstrate, that the incorporation of specific prior knowledge leads to an improved estimator behaviour; for example, reduced variance and unbiased estimates. We implemented laboratory experiments in order to analyse the presented approach for the application in real pneumatic conveying processes. We demonstrate the improved robust estimation behaviour by means of comparative reconstruction results obtained with different algorithms and priors. Furthermore, the uncertainty of the estimated volume fraction is analysed in steady state conveying processes. Hereby, it is demonstrated, that appropriate prior information improves the estimation performance also for measurements coming from real pneumatic conveying processes, making ECT a suitable tool for the volume fraction estimation in such transport systems.
Keywords
Introduction
Pneumatic conveying is a standard technique for the transport of particulate and granular materials (Klinzing et al., 2011). It is used in various industries including agriculture and food industries; for example, the transport of wheat or flour – or heavy and chemical industries; for example, the transportation of cement, and so forth (Kraume, 2012). In pneumatic conveying, the material is transported by means of a gas stream through a pipe system. The transport process is characterized by means of the spatial material distribution of the particulate material within the transport pipe. Figure 1 sketches different flow regimes for pneumatic conveying and the relation for pressure drop and gas velocity (Jama et al., 2000). For high stream velocities of the transport gas, the material is uniformly distributed over the cross section of the transport pipe. The density of the material stream is low, the flow regime is referred to as dilute or dispersed flow. For decreased gas velocities the flow regime shows a distinct material layer moving at the bottom of the pipe with a dilute phase above. Flow profiles showing this distinct bottom layer are generally referred to as stationary flows. Due to the decreased pressure drop these flow regimes are favourable because of the reduced energy demands. For further decreased gas velocities the material moves by means of a concentrated material bulk.

Flow regimes for pneumatic conveying (Jama et al., 2000).
The efficient operation of a pneumatic conveying systems requires the continuous determination of certain flow parameters such as the volume flow or the mass flow. The volume flow
where
Assuming a uniform velocity distribution with velocity
where
and
In this paper, we focus on the determination of
The comparatively low permittivity values of the materials used in pneumatic conveying processes (Kraume, 2012) enable the application of linear reconstruction algorithms (Neumayer et al., 2011b). For this reason and since computational costs are an immanent issue for the continuous determination of flow parameter by means of ECT, we investigate the estimation of
This work is a technically extended version of the conference paper (Suppan et al., 2018) the authors presented at the
Extension of the sample-based prior presented in Suppan et al. (2018) to improve the robustness of the volume fraction estimation approach in real pneumatic conveying processes by means of the implementation of robust priors.
Demonstration of the improved estimation behaviour by means of comparative reconstruction results from lab experiments obtained with different priors.
Uncertainty analysis of the estimation result for the application of the presented approach in real pneumatic conveying processes. Hereby, steady state flow conditions are generated on a test rig.
For the application in real pneumatic conveying systems, the presented sample-based prior approach is extended in order to improve the robustness of the estimates with respect to variations in the flow profiles. The reconstruction behaviour of different estimators and priors is analysed by means of a time varying horizontal conveying process. The necessity of a proper robust prior is addressed when it comes to the reconstruction of material distributions in real conveying processes. The uncertainty of different estimators and different priors is analysed in order to show the improved estimation performance of the presented approach. This analysis is implemented for steady state conveying processes, where the material stream has a constant mass flow rate with a constant velocity and therefore also a constant volume fraction. For the analysis of the uncertainty the standard deviation of the estimated volume fraction is calculated for stationary flow conditions. These experimental results are compared with the findings of the simulation study.
This paper is structured as follows. In Section II, we will briefly discuss ECT. In Section III, we will present the design of the sample-based prior and demonstrate the behaviour of different prior distributions in simulation studies. The laboratory experiments are presented in Section IV.
ECT
In this section, we briefly discuss the sensing principle and the simulation model of ECT and the inverse problem for image reconstruction. Figure 2 depicts the scheme of an ECT sensor. The sensor consists of several electrodes, a non-conductive pipe and a shield. The electrodes are placed on the outer circumference of the pipe. The capacitances between the electrodes are influenced by the dielectric properties of the materials inside the pipe (Brandstätter et al., 2003b; Holder, 2005; Neumayer et al., 2011b). An ECT measurement system determines the capacitances between the electrodes using suitable circuitry (Wegleitner et al., 2005, 2008). The shield guards the sensor from external influences.

Scheme of an ECT sensor.
The inverse problem of ECT refers to the estimation of the spatial dielectric material distribution from the capacitance measurements. This step requires a simulation model of the sensor. To simulate the sensor, the governing partial differential equations have to be solved by an appropriate numerical technique. Electric fields inside the ECT sensor are governed by the potential equation
Inverse problem and prior information for pneumatic conveying
The inverse problem of ECT is of severe ill-posed nature (Hansen, 1998). To obtain a stable result specific measures have to be applied. Within the Bayesian framework or statistical inversion theory, prior information is incorporated into the estimator design (Kaipio and Somersalo, 2005). Statistical inversion theory considers any variables to be random variables. The characterization is based on probability density functions (pdfs)

Exemplary samples from a rod-type prior distribution.

Exemplary samples from a Gaussian-type prior distribution.
State reduction
A further technique to incorporate prior information to the solution of the inverse problem is given by the approach of a state reduction (Neumayer et al., 2019). Given an ensemble of prior samples, a state reduction of form
Linear image reconstruction algorithms
In this section, we briefly address the design of estimators, or reconstruction algorithms within the Bayesian famework (Cui et al., 2016; Watzenig and Fox, 2009). Most materials of particulate flows have a comparatively low relative permittivity (Kraume, 2012). Due to this the forward map can be approximated by
In combination with the state reduction, the estimator becomes (Neumayer et al., 2018a)
Both estimators fall into the class of linear back projection algorithms, as the computation requires a single matrix vector multiplication.
It has been demonstrated, that the incorporation of a state reduction incorporates prior information to algorithms due to the intrinsic information of the basis vectors. This involves a stabilization of the ill-posed inverse problem without the necessity of an explicit prior distribution
Further, algorithms (4), (5) and (6) can be extended by state constraints to avoid infeasible estimation results; for example,
A further back projection type reconstruction algorithm of form
Estimation of
Given an estimate
Hereby,
Design of specific prior information for flow profiles and analysis of the estimation behaviour
The concept of sample-based priors can be adapted for flow regimes in pneumatic conveying systems (Neumayer et al., 2018b). In this section, we address the design of specific sample-based prior information for flow patterns occurring in pneumatic conveying systems and we analyse and compare the estimation behaviour of different algorithms and different priors.
Prior design
The aim of this subsection is the construction of specific prior information for pneumatic conveying systems. In order to achieve this, the flow regimes depicted in Figure 1 are analysed. The different flow regimes can be summarized by three main cases. The first case is given by dilute flow regimes where the particles are distributed over the whole cross section of the pipe with a low density. In the second case a distinct bottom layer of a dense phase and a dilute phase in the upper domain of the pipe is present. The third case is given by the slug flow regime, where the whole cross section of the pipe is filled with dense bulk material. A sample-based prior for these material distributions is given by random samples of a two-dimensional cross sectional representation of the different flow regimes.
Horizontal flow samples with even boundaries between the phases
In the simplest cases, the random samples are generated by the parametrized material distribution depicted in Figure 5. The material distribution is given by a dense bottom layer with a certain height

Parametrization for horizontal flow profiles.
Horizontal flow samples with uneven and smooth boundaries between the phases
In order to generate a prior, which is robust against deviations in the flow profiles, a more complex representation of the different flow regimes is given by the parametrized material distribution depicted in Figure 6(a). Hereby, the boundary between the two phases is uneven and has smooth behaviour. In Guan et al. (2011) it is demonstrated that this kind of flow profiles can occur in horizontal pneumatic conveying processes. The dilute flow regime and the dense slug flow regimes are generated in the same way as discussed previously. The flow regimes with a distinct bottom layer are in this case parametrized by three heights –

Parametrization of uneven horizontal flow patterns used to improve the robustness against deviations in the flow profiles and an ensemble of exemplary randomly generated boundaries between the dense and the dilute phase.
Simulation study to analyse the behaviour of different priors
In this subsection, we analyse the estimation behaviour of different algorithms with respect to the prior information. We compare the rod-type and Gaussian-type prior for arbitrary material distribution with specific prior information for flow patterns. In order to analyse the estimation performance, we use the evaluation framework depicted in Figure 7. The evaluation maintains two sets of ensembles, which are evaluated on different simulation models for the sensor. For the generation of simulated data and the determination of the true parameter

Framework for the analysis of different reconstruction methods.
Dimensions of the ECT sensor and simulation setup
Figure 8(a) depicts a photograph of a lab test rig with an ECT sensor. It is used to perform flow experiments with particulate materials and simultaneously acquire ECT measurements. The dimensions of the ECT sensor, which is used in the simulation study is the same as the sensor of the lab test rig. The inner radius of the process pipe is given by

Lab test rig with ECT sensor and SNR measurement.
The number of eight electrodes for the lab sensor and the study was selected by the authors, as we are interested in monitoring of particulate flows with capacitive sensors, while keeping the instrumentation effort low. The capability for flow monitoring with a reduced number of electrodes has been presented in Neumayer and Bretterklieber (2014), where an ECT sensor with only five electrodes is used. For arbitrary material distributions, various articles suggesting 12 or 16 electrodes have been presented. The capability to reconstruct flow profiles with an ECT sensor with a lower number of electrodes is due to the specific structure of flows, which is addressed by the prior design. A fewer number of electrodes allow a sensor design with larger electrodes and therefore increased coupling capacitances between the electrodes, which generally leads to improved signal to noise ratios (SNR).
Figure 8(b) depicts an SNR measurement of the lab ECT sensor. The SNR is indicated with respect to the total signal change between an empty measurement and a measurement for the sensor filled with particulate polyethylene pellets with
Statistical evaluation of the estimation error
For the evaluation of the reconstruction algorithms we analyse the estimation error
Figures 9 and 10 depict the simulation results obtained with the OSOA algorithm and the linearized MAP estimator (LMAP), respectively. The plots show the mean

Mean

Mean
For the linearized MAP estimator also, the variance is decreased over the whole range of

Overall mean
Test rig measurements and lab demonstration
This section contains a demonstration of the improved estimation behaviour of the presented approach with measurements coming from the lab test rig. A photograph of the lab test rig setup is depicted in Figure 8(a). It contains a hopper filled with particulate polyethylene pellets with a relative permittivity of
Reconstruction experiments
In this subsection, we demonstrate the reconstruction behaviour of linear back projection type estimators with different priors for measurements coming from lab experiments. Additionally, we analyse the required reconstruction times of different algorithms. Hereby, a horizontal pneumatic conveying flow is generated where the material stream decreases with time. After initiating the flow by the opening of the valve the hopper is gradually emptied due to the gravitational flow of the particulate material. At a certain time instant pressurized air is injected in the pipe system. This gas injection causes increased velocities of the particles and a simultaneous decrease of the volume fraction. Figure 12 depicts camera recordings of the flow experiment at different time instants. Figure 12(a) shows the flow state before the pressurized air is injected. Here, the whole cross section of the pipe is filled with bulk material. Figure 12(b) depicts the flow state at the beginning of the gas injection. The gas stream creates a dilute upper phase. The photograph shown in Figure 12(c) depicts the flow state at a later time instant where the hopper is emptied.

Camera recordings of the flow experiment at different time instants.
Figure 13 depicts exemplary sequences of reconstruction results obtained by the linearized MAP estimator with different priors. Figure 13(a) depicts the reconstructed images obtained by the incorporation of rod-type prior information. These images show distinct artefacts in the dense phase as well as in the dilute phase. The reconstruction with rod-type prior information does not allow the representation of homogeneous and constant material distributions. Figure 13(b) depicts the images obtained with Gaussian-type prior information. These results suffer from the same issues than the results obtained with the rod-type prior. The artefacts however are less distinct and the material distribution shows a smoother behaviour. Figure 13(c) depicts the reconstruction results obtained by means of the flow-type prior. The reconstructed images show distinct minima in the dense flow phase as well as artefacts in the dilute flow phase. This result suggests that the flow-type prior depicted in Figure 5 is too simplistic to provide meaningful reconstruction results for real pneumatic conveying processes. Other linear back projection type estimators – for example, the OSOA algorithm – show similar behaviour when it comes to the reconstruction of real flow experiments. Figure 13(d) depicts the sequential reconstruction results achieved with the linearized MAP estimator and the robust-flow-type prior. The use of this prior information involves a smoother behaviour of the reconstruction results with a more homogeneous distribution of the permittivity in the dense phase as well as in the dilute phase. Also, the appearance of artefacts in the reconstructed images is significantly reduced. This demonstrates the advantages of the incorporation of appropriate prior information to the estimation task.

Reconstruction results of the linearized MAP for a flow experiment at different time instants using different prior distributions.
Computation times
Regarding computation times, reconstruction rates of about 150 Frames/s for the back-projection algorithms like the OSOA and the linearized MAP estimator were achieved. When applying state constrains the frame rate is reduced to 10 Frames/s. The results were computed with MATLAB2017 on an Intel Core i7-4510u CPU with 2x2 GHz clock rate.
Uncertainty analysis by means of steady state conveying experiments
In this subsection, we present a measurement-based analysis of the uncertainty of different reconstruction algorithms and prior distributions. The test rig is used to produce horizontal steady state flows with a constant particle velocity

Scale-based mass signal and estimated volume fraction
Figure 15 depicts an analysis of the standard deviation of different reconstruction experiments, where each trend represents the results for a single flow experiment and each sub-figure represents a different estimator. We maintain the same representation of the uncertainty as depicted in Figure 11(b). The results show the improvement in the reduction of the standard deviation, due to the use of an appropriate prior. The evaluated standard deviations for the measurements are yet higher than the simulated standard deviations; for example, the results depicted in Figures 9, 10 or Figure 11(b). We consider this increase to be caused by variations inside the transport process of the measurement experiment – for example, local density variations – which are yet not modeled by the priors.

Analysis of the standard deviation
Figure 16 depicts the mean standard deviation

Mean standard deviation
Conclusion
In this paper, we presented the estimation of the volume fraction in pneumatic conveying systems from capacitive sensor data using ECT. We addressed the construction of prior information and the modification of different tomographic reconstructions methods. We presented a framework for the systematic analysis of the different algorithms and demonstrate the advantages of incorporating specific prior information for flow profiles in pneumatic conveying processes; for example, unbiased estimates and reduced variances. The presented approach was also applied to measurements coming from a lab test rig in order to demonstrate the improved and robust estimation behaviour also for data coming from real measurements. Comparative reconstruction results show an improved image quality and representation of the true material distribution within the conveying process, when applying specific prior information. The results achieved in the lab experiments also demonstrate the improved estimation behaviour regarding the uncertainties of the estimates when applying the demonstrated approach. The achieved results show the capability of tomographic signal processing methods for flow parameter estimation in pneumatic conveying systems.
Footnotes
Acknowledgements
The authors would like to thank Mr Thomas Wiener for his support during the lab experiments.
Declaration of conflicting interests
The author(s) declared no potential conflicts of interest with respect to the research, authorship, and/or publication of this article.
Funding
The author(s) disclosed receipt of the following financial support for the research, authorship, and/or publication of this article: This work is funded by the FFG Project (Bridge 1) TomoFlow under the FFG Project Number 6833795 in cooperation with voestalpine Stahl GmbH.
