Abstract
Drilling of carbon fiber-reinforced polymer (CFRP) is widely employed in manufacturing processes in the aeronautical, automobile, and energy industries. The evaluation of the hole region focusing on wall roughness and delamination phenomena is extremely important to predict bolted joints' performance, where at least one of the adherent is a composite material. Thus, this work performed a statistical analysis on the delamination (entrance and exit of the plate) and wall roughness of drilling holes in an 8.6 mm thick CFRP plate carried out by an uncoated carbide drill under compressed air-cooling, varying the cutting speeds and feed rates. Since air-cooling usage combines positive aspects, such as low-cost implementation and shorter process time compared to ultrasonic-assisted drilling, it turns out to be an excellent alternative for aeronautical industry. Thus, the main contribution of the present work consists on analyzing the variation of the delamination in the entrance and exit of the first and tenth holes of a CFRP plate after dry and air-cooled drilling. This variation of the delamination between the cold drill (first hole) and the heated drill due to the drilling holes' sequence (after ten holes) is investigated for 18 different combinations of parameters (runs). For instance, it is shown that if the combination of parameters values is suitable, then it is possible to reduce the mean value of adjusted delamination factor for the entrance of the tenth hole around 11% when comparing cooled-air with dry cutting.
Introduction
Aeronautical, automobile and energy industries are the major boosters of composite materials application. They are focused on developing these materials to achieve better mechanical properties combining self-weight reduction, which decreases energetic costs and, consequently, reduction of pollutant gas emissions into the atmosphere. For instance, the Boeing 787-Dreamliner and the Airbus A350 possess around 50% of their weight composed of composite materials, mainly CFRP (carbon fiber reinforced polymer) parts. 1 Fasteners can join those composite parts, which require holes to assembly composite and metallic structures by using screws or rivets. However, high precision and low tolerances are critical issues during the drilling process, especially in the aeronautical industry. 2 In Airbus A350, more than 55 thousand holes are necessary, 3 producing demountable unions. 4 These holes are commonly made by drills 5 or milling cutters, 6 usually with a carbide tool.7,8 In the particular case of drilling CFRP, the tools can fastly wear out due to the high toughness and stiffness of composite materials. 9 Besides, delamination and cracks can occur in the composite parts during the process, mostly with the increase of the tool wear.3,10
Considering the drilling of composite materials, there are four main types of defects, which occur during the process using helical drills in laminated composite materials, which can be identified as follows: (1) damage at the entrance of the hole (tool entrance); (2) damage at the exit of the hole (tool exit); (3) dimensional defects and (4) thermal defects. 11 The present work focuses on the evaluation of the first two types of defects. The damage at the hole entrance is related to the fiber debonding of the first layer due to the drill cutting edges, and this can induce delamination. In this case, the material tends to be pulled by the drill's helix (peel-up). The damage at the hole exit is due to the compression stress components caused by the thrust force at the bottom layers. When the stress state exceeds the fiber-matrix adhesion strength, initiation and propagation of cracks occur, resulting in further delamination. Hence, the material tends to be pushed (push-down), and this type of damage is harder to be avoided. 12 Furthermore, the CFRP's flexure strength decreases with the increase of the delamination area after drilling. 3 In addition, some fibers can be uncut, requiring further machining even if it does not affect the mechanical properties of the final part. 13
Regarding the scenario pointed above, different techniques have been used to detect the delamination degree, both in the hole entrance and exit. Davim and Reis
14
used microscopy to evaluate the delamination promoted by drilling of CFRPs. Chen
15
proposed the delamination factor concept (
Another important issue consists on thermal defects, which can be created due to the friction between the drill and the composite material. This affects the polymer matrix integrity and being deleterious to the finishing of the hole wall surface. In fact, the quality of the hole wall surface can be also affected by the formation of cutting chips, which consist of a group of fragile fractures that are strongly dependent on the fiber's orientation. 17 Since the fracture of composites does not require large amounts of energy than shear failure in metals, the cutting force and temperature required in CFRP machining are much lower than their metal counterparts. 18 Thus, for the CFRP machining process, it is possible to eliminate the possibility of occurring diffusion and/or dissolution wear mechanisms. 19 However, as commented earlier, the temperatures can still affect the material properties mostly of the polymer matrix, 20 increasing local damages, such as debonding and pull-out of fibers. 4 Besides, the temperatures can reach values beyond the glass transition temperature of the polymer matrix at high cutting speeds. In these cases, the softened polymer and the carbon fibers can create irregular surfaces. 21 In general, the machined hole quality reduces with temperature increases, and therefore, it is predicted that the quality shall increase with temperature reduction. The increase of the temperature during the drilling process causes matrix stiffness reduction, resulting also in global damages, such as delamination, transverse cracking, and others. 22 By one hand, one way to overcome this issue is to reduce the temperature at the hole's region using compressed air-cooling during the drilling operation aided by a vortex tube. 23 However, on the other hand, it is worth noting that the chip generated when machining CFRP can be in the form of fine particles, 24 and these particles can be suspended, causing danger to the operator, 25 mostly using compressed air-based cooling systems.
In spite of the problem described above, air-cooling usage combines positive aspects, such as low-cost implementation and shorter process time compared to ultrasonic-assisted drilling. Thus, it turns out to be an excellent alternative for aeronautical industry, where compressed air-cooling drilling of CFRP parts should be carried out in machine tools' area enclosed, mainly with an exhaustion system. Therefore, by using a machining center with an enclosed machining area, different values of combination of process parameters are investigated to evaluate delamination degree via adjusted delamination factor (
Materials and methods
Experiments were performed at a Romi Discovery 308 machining center with an enclosed machining area, 5.5 kW maximum power, and 4000 rpm maximum rotation. A CFRP plate with an 8.6 mm thickness manufactured by hand layup technique was used during the tests. The reinforcement was a bidirectional (BD) carbon fabric with pre-impregnated epoxy resin stacked as a
CFRP’s plate: Prepreg material and geometry data.
aSimilar material.

(a) Polymer support plate; (b) Setup of the experimental test.
The drill holes were machined by a Sandvik CoroDrill 860 H10F NM, an uncoated twist solid carbide drill with a 6.0 mm diameter, cross edging, 130° point angle, and 16.6° helix angle. The compressed air-cooling was produced by a Turbo Air Eurotools FTA-12-MC vortex tube connected to a 3 bar (300 kPa) air-line, resulting in a 6 degrees Celsius output temperature. The axial run-out error of the drill (δ) was assessed using a Starrett dial gauge with a resolution of 1.0 μm. The setup of the experimental test is shown in Figure 1(b).
A full-factorial design of experiments (DOE) was carried out considering the variation of cutting speed (vc = 25, 50, 75 m/min) and feed rate (f = 25, 50, 75 µm/rev.) to compare the dry condition at room temperature (25 °C) with the air-cooled condition in CFRP drilling. Therefore, this procedure results in 32⋅21 = 18 combinations of parameters (runs). Moreover, ten holes were drilled for each condition, resulting in 180 holes (Table 2).
Experimental parameters.
The adjusted delamination factor was analyzed in the entry and exit of the first and tenth holes after dry and air-cooled drilling for each run (Figure 2) to verify the variation of the delamination between the cold drill (first hole) and the heated drill due to the drilling holes' sequence (after ten holes).

Delamination analysis: first and tenth hole (entry and exit).
After drilling, images were obtained from the first and the tenth holes made in each run using a portable digital microscope Dino-Lite Pro model AM-413ZT with 50x amplification at the entrance and the exit of the drill in the CFRP plate. Essentially, those images were used for analyzing the presence or not of delamination. Based on the recorded images, the damaged area (
The roughness values of the first hole drilled (cold drill) at each condition were determined through the average of three measurements performed by a Mitutoyo Surftest SJ-201P portable stylus equipment with 0.01 µm resolution, using a sampling length of le = 0.8 mm and an evaluating length of lm = 4 mm. Moreover, the 2CR75 filter was used to generate the roughness parameters Ra (average roughness), Rq (root mean squared roughness), Rz (average maximum peak-to-valley height), and Rt (total roughness). In fact, based on the literature, it is expected that the parameter Rt presents the same tendency as Ra, being the most adequate for the CFRP investigations, because it can describe an average roughness and is still sensitive to fiber debonding. 26
Besides, additional images were obtained using a scanning electron microscope (SEM) Zeiss Evo Ma10 for improving the analysis of the hole's wall surface. It was necessary to use a Bal-tec SCD 050 thermal spray coating machine to create a thin gold skin over the surfaces.
Lastly, the variance analysis (ANOVA) of the obtained data was performed using the Minitab 18 software. It is a method to test the equality between three or more populational averages based on the sample variance analysis. According to Montgomery,
27
to perform the analysis mentioned above is necessary that the quality of model fit would be sufficient; this is given by the coefficient of determination (R2) above 70%. Therefore, as closer to 100% R2 is, as greater the regression reliability, ensuring the statistic model's suitability and indicating low variability in the proper response results. Moreover, a confidence interval of 95% (p-value ≤ 0.05) was considered. The ANOVA of the results was performed to verify the influence of the controllable factors (cutting speed (vc), feed rate (f), and cooling condition (cc)) on the adjusted delamination factor in the entry (
Results and discussions
The results present the calculated delamination factor, the measured roughness values, and the performed variance analysis (ANOVA). It is worth mentioning that the tool flank wear (VB) was verified throughout the study. However, the measured wear was negligible even after the execution of all 180 holes.
Figure 3 presents the adjusted delamination factor values generated at the holes entrances (

Adjusted delamination factor at the entrance of the first and tenth holes of each run.

Adjusted delamination factor at the exit of the first and tenth holes of each run.
The hole wall roughness was investigated by evaluating four parameters: Ra, Rq, Rz, and Rt. Ra and Rq values are depicted in Figure 5, while Rz and Rt are shown in Figure 6. More details about the hole wall roughness analysis are presented based on the ANOVA.

Ra and Rq values of the first hole wall surface of each run.

Rz and Rt values of the first hole wall surface of each run.
The analysis of measured
ANOVA of the results.

Main effects plots regarding the adjusted delamination factor.

Main effects plots regarding the roughness parameters for the first hole.
The analyses of delamination showed that the level of damage at the hole entrance (
The compressed air-cooling usage significantly reduced the
For
For
Still for
When comparing
Examples of differences of induced delamination between the first and tenth holes and between dry and cooled-air conditions are observed in Figure 9, which shows the entrance of the holes for runs 4 (dry cutting with vc = 50 m/min and f = 25 µm/rev.) and 13 (cooled-air cutting with vc = 50 m/min and f = 25 µm/rev.). It is verified that the reduction of the plate stiffness (after nine holes) increases the peel-up occurrence, increasing the

Images of the holes entries.
The
Four runs under air-cooled condition had the lower
Regarding the
The air-cooled condition increases the maximum delamination diameter at the hole exit. The fibers remained stiff and were warped in a region far from the hole edge, increasing the push-down occurrence. Nevertheless, the cooled-air reduces the occurrences of uncut fibers (Figure 10), as demonstrated by Koklu et al. 38

Comparison of the delamination and uncut fibers at the exits of the first holes for runs with vc = 75 m/min and f = 75 µm/rev.: (a) dry; (b) air-cooled.
The ANOVA of the roughness parameters indicated that, for a 95% confidence interval, the only significant influence over Rz is cc (64.8%). Besides, the combination of vc x cc was partially significant, with 18.4% of contribution. Considering total roughness (Rt), cc (46%), and the combination of vc x cc (22.1%) presented significant influences on Rt values. As explained earlier, the Ra and Rq parameters that did not reach R2 > 70% were unconsidered. However, the parameter Rt can be useful to evaluate the surface quality. 26
The increase of cutting speed (vc) harmed the surface quality because the CFRP plate used is thick, contributing to the temperature growth in the cutting zone. Thus, it increased the surface quality's adverse effects, justifying the compressed air-cooling as the most influential factor for hole wall roughness. These results agree with those observed by Abish et al. 37
During the dry drilling, the lower cutting speed (vc = 25 m/min) produced better results compared to the others vc tested due to the lower temperatures,22,39 and thrust forces developed, 32 which reduce the damage. Consequently, the increase of vc makes the temperature rise, which harms the surface. It is noted that run 9 (vc = 75 m/min) generated better results than the other dry runs and similar results using cooled-air. El-Hofy et al. 40 argued that this phenomenon is due to the higher feed rate (f = 75 µm/rev. in run 9) that reduces the temperature generated by high cutting speed combined with plate thickness.
For the runs with higher vc and f, the compressed-air cooling (runs 13 to 17) resulted in lower roughness values compared to dry cutting (runs 4 to 8), showing up to 58% of decrement for Ra, 52% for Rz, 57% for Rq and 57% for Rt. The air-cooled condition reduced the damage related to the temperature for high speeds, which generated better results since the high speed is beneficial to the hole wall roughness.26,41 Joshi et al. 35 and Abish et al. 37 also obtained lower roughness values using air-cooled than dry drilling. Run 18 had similar results to run 9, with a slight reduction in the values of roughness parameters in comparison with dry cutting (5% for Ra, 11% for Rz, 7% for Rq and Rt) due to high cutting speed and feed rate (vc = 75 m/min and f = 75 µm/rev.). Joshi et al. 35 observed that the cutting zone's temperature negatively affects the surface finish for high cutting speed because the cooled-air could not reduce the temperature, showing similar results when in dry drilling.
Figure 11 shows SEM images of the holes' walls for runs 4 (dry) and 13 (air-cooled). It is noticed a high variation between dry and air-cooled drilling. Various cavities were identified in dry drilling, as well as fiber pull-out from the matrix, with high variation between the laminate plies. A high degradation of the polymer matrix in dry drilling is noticed, presenting the fibers exposed without polymer matrix. This difference between the machined surfaces using dry and air-cooled drilling was observed, not only for runs 4 and 13, but also in all runs for vc = 50 and 75 m/min.

The inner wall surfaces in the first holes for vc = 50 m/min and f = 25 µm/rev.
Low temperatures facilitate the occurrence of fibers' breakage since they reduce their resilience under air-cooled. These ruptures avoid the pull-out phenomenon, generating fewer rough surfaces after drilling. In this case, the occurrence of fiber pull-out generates high cavities on the surface. In dry drilling, the fiber pull-out and the fiber-matrix separation increase with the temperature, deteriorating the machined surface.4,35,37,42,43
Another observation about the hole wall roughness was the high variability in the same hole for three measurements with different profiles found. Eneyew and Ramulu 26 explained that these variations could occur in locations where the carbon fibers pulled out, creating valleys, splinters, and cracks.
Figure 12 shows the lowest and the highest roughness values for the three measured profiles considering runs 4 (dry) and 13 (air-cooled) in the drilling with vc = 50 m/min and f = 25 µm/rev. Figure 12(a) presents the high variability observed for dry drilling. Also, the air-cooled condition results showed similar roughness profiles throughout the hole wall surface (Figure 12(b)).

Roughness values of the inner hole wall: (a) the highest values for run 4; (b) the lowest values for run 13.
Figure 13 presents the runs 6 (dry) and 15 (air-cooled) with vc = 50 m/min and f = 75 µm/rev., showing the differences between the first and tenth holes. It is observed that for both runs (dry and air-cooled), the surface damage increases with the number of uninterrupted holes, probably due to the cumulated heat. This phenomenon is analogous to delamination occurrences.

Differences on the wall surfaces of runs 6 and 15 between the first and tenth hole, vc = 50 m/min, and f = 75 µm/rev.
Conclusions
The present work investigated delamination and hole wall quality of CFRP plate drilling under different cooling conditions (cc), cutting speeds (vc), and feed rates (f). After measuring data to calculate the adjusted delamination factor ( Regarding the Concerning Regarding the hole wall roughness, higher vc values improved its quality but provided worse results for
Finally, on the one hand, the compressed air-cooling application reduced the delamination at the entrance (which is confirmed by the literature 44 ) of the holes. Therefore, the hole wall roughness is improved since the fibers' resilience is modified due to the air-cooled, facilitating the drilling and reducing the fiber pull-out and damage due to high cutting speeds. On the other hand, the delamination at the hole exit is increased when push-down effects increase compared to dry cutting. This may occur due to the change in the material properties, mainly polymer matrix, under low temperatures. However, the variation of cutting speed (vc) combined to the variation of feed rate (f) (at the same time) in drilling is a promising alternative to decrease the delamination at the hole exit. Thus, if small values for vc are used during the hole opening, and, after that, values of vc are increased and values of f are reduced when the drill point approaches to the end of the drilled hole, then better results can be obtained in terms of reduction of delamination.
Footnotes
Declaration of Conflicting Interests
The author(s) declared no potential conflicts of interest with respect to the research, authorship, and/or publication of this article.
Funding
The author(s) disclosed receipt of the following financial support for the research, authorship, and/or publication of this article: The authors thank Sandvik Coromant Co. for the cutting tool, Green Service Co. for the vortex tube, and CAPES (grant no. 88882.346387/2019-01) and CNPq (process no. 310656/2018-4 and 134587/2018-9) for financial support.
